9 edition of Nuclear magnetic resonance in solid polymers found in the catalog.
Includes bibliographical references (p. -336) and indexes.
|Statement||Vincent J. McBrierty and Kenneth J. Packer.|
|Series||Cambridge solid state science series|
|Contributions||Packer, K. J.|
|LC Classifications||QD139.P6 M38 1993|
|The Physical Object|
|Pagination||xxii, 347 p. :|
|Number of Pages||347|
|LC Control Number||92045158|
Nuclear magnetic resonance (NMR) spectroscopy may now be the most valuable tool for elucidation of molecular structure, order and dynamics. As far as macromolecules are concerned, NMR is Author: Hans Wolfgang Spiess. Polymers The world polymer industry continues to grow as new applications and new materials are developed. Whether for common commodities such as polystyrene or PVC or for a more exotic wax-modified polymer system, there is the need for rapid quality control testing methods to ensure reproducible and environmentally friendly products.
NUCLEAR MAGNETIC RESONANCE IN SOLID POLYMERS VINCENT J. McBRIERTY Professor of Polymer Physics, Trinity College, Dublin and KENNETH J. PACKER Chief Scientist, British Petroleum Co. p.l.c. Щ CAMBRIDGE ШЖ UNIVERSITY PRESS. This informative publication presents the broad application of nuclear magnetic resonance to many of today's problem areas in agriculture. Solid-state NMR methodology is covered, with its applications to the study of intact agricultural matrices such as plant cell walls, photosynthetic chloroplast membranes, forages, wood cellulose, and soils.
Individual chapters, written by leaders in the development and application of NMR from around the world, treat systems that range from synthetic polymers, liquid crystals, and catalysts to proteins and oligonucleotides and techniques that include deuterium NMR, magic angle spinning, multidimensional spectroscopy, and magnetic resonance imaging. Nuclear Magnetic Resonance There are various energy levels for the nucleus with a magnetic moment in a static magnetic field. The nucleus will undergo a transition if an electromagnetic wave with a frequency given by Eq. () is used. This transition is nuclear magnetic res-onance (NMR). Thus the fundamental equation can be derived as follows:File Size: KB.
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‘This book provides an excellent overview of the breadth of solid-polymer problems that have been addressed with NMR written by authors who have helped this field mature over the past 25 years.
It is a resource that will be valuable to the practising NMR spectroscopist, as well as those interested in the solid properties of polymers ’Cited by: Nuclear magnetic resonance in solid polymers.
[Vincent J McBrierty; K J Packer] Advanced Materials 'This book provides an excellent overview of the breadth of solid-polymer Read more User-contributed reviews # Nuclear magnetic resonance spectroscopy\/span>\n \u00A0\u00A0\u00A0\n schema.
Nuclear Magnetic Resonance in Solid Polymers by Vincent J. McBrierty,available at Book Depository with free delivery worldwide. Solid-state NMR (ssNMR) spectroscopy is a special type of nuclear magnetic resonance (NMR) spectroscopy, characterized by the presence of anisotropic (directionally dependent) interactions.
Compared to the more common solution NMR spectroscopy, ssNMR usually requires additional hardware for high-power radio-frequency irradiation and magic-angle spinning. This book provides an up-to-date and comprehensive overview of the fundamentals of NMR, with applications of multidimensional NMR and the new solution and solid-state methods in polymer science.
NMR of Polymers is written by leading authorities for graduate students and professionals in. This book is an authoritative and comprehensive account of the principles and practice of modern NMR spectroscopy of solid polymers to determine their structure and dynamics at a molecular : Ulrich Scheler.
Nuclear Overhauser effects can sometimes be observed for solid polymers, particularly for those near or above the glass transition temperature.
Such measurements are also difficult to interpret in terms of the molecular motions because they are also mainly due to methyl group rotation (46). A recent method to perform spatially resolved nuclear magnetic resonance (NMR) and relaxation measurements in narrow slices of a solid is applied to the study of the mobility changes of polymer.
Nuclear Magnetic Resonance Spectroscopy [John H. Nelson] on *FREE* shipping on qualifying offers. This is the only how-to volume that investigates the spectroscopy of a variety of nuclides other than H and C in depth.
It contains extensive reference material and numerous problemsCited by: Nuclear magnetic resonance spectroscopy, most commonly known as NMR spectroscopy or magnetic resonance spectroscopy (MRS), is a spectroscopic technique to observe local magnetic fields around atomic sample is placed in a magnetic field and the NMR signal is produced by excitation of the nuclei sample with radio waves into nuclear magnetic resonance, which is detected with sensitive.
Find many great new & used options and get the best deals for Cambridge Solid State Science: Nuclear Magnetic Resonance in Solid Polymers by Kenneth J. Packer and Vincent J. McBrierty (, Paperback) at the best online prices at eBay. Free shipping for many products. CHAPTER 12 Nuclear Magnetic Resonance Spectroscopy of Living Systems By M.
Prior,CHAPTER 13 Nuclear Magnetic Resonance Imaging By T. Watanabe,CHAPTER 14 NMR of Paramagnetic Species By R. Sharp,CHAPTER 15 NMR of Liquid Crystals and Micellar Solutions By A. Khan and A.
Caria,Author Index, ,Pages: Chapter Nuclear Magnetic Resonance (NMR) Spectroscopy direct observation of the H’s and C’s of a molecules Nuclei are positively charged and spin on an axis; they create a tiny magnetic field + + Not all nuclei are suitable for NMR.
1H and 13C are the most important NMR active nuclei in organic chemistry Natural Abundance 1H % 13C %. Nuclear Magnetic Resonance Probes of Molecular Dynamics, Robert Tycko (Ed.), Kluwer Academic, Dordrecht (). Google book. Nmr Techniques In Catalysis, Alexis T.
Bell and Alexander Pines (Eds.), Marcel Dekker, New York (). Google book, BookZz. Nuclear Magnetic Resonance in Solid Polymers, Vincent J.
McBrierty and K. Packer. Abstract. A simple introduction to nuclear magnetic resonance in solid polymers is given. The basic theory of the n.m.r. phenomena of importance (dipole-dipole coupling, chemical shift anisotropy and magnetic relaxation) is described, and the application of these effects to polymers is illustrated by selected by: 2.
The journal Solid State Nuclear Magnetic Resonance publishes original manuscripts of high scientific quality dealing with all experimental and theoretical aspects of solid state NMR. This includes advances in instrumentation, development of new experimental techniques and methodology, new theoretical insights, new data processing and simulation.
Nuclear magnetic resonance (NMR) is a method of physical observation in which nuclei in a strong constant magnetic field are perturbed by a weak oscillating magnetic field (in the near field and therefore not involving electromagnetic waves) and respond by producing an electromagnetic signal with a frequency characteristic of the magnetic field at the nucleus.
As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to Pages: Nuclear Magnetic Resonance.
Paperback – January 1, out of 5 stars 1 rating. See all 4 formats and editions Hide other formats and editions. Price New from Used from Hardcover "Please retry" $ — $ Paperback "Please retry" $ 5/5(1). ISBN: OCLC Number: Description: xviii, pages: illustrations ; 25 cm: Contents: Introduction --Principles of NMR of organic solids --High-resolution NMR techniques for solids --Fourier theory for 1D and 2D NMR --Short review of structure and dynamics of solid polymers --Multidimensional separation and correlation --Polymer dynamics: multidimensional.
Nuclear magnetic resonance crystallography (NMR crystallography) is a method which utilizes primarily NMR spectroscopy to determine the structure of solid materials on the atomic scale. Thus, solid-state NMR spectroscopy would be used primarily, possibly supplemented by quantum chemistry calculations (e.g.
density functional theory), powder diffraction etc.DNP samples are prepared by adding a polarizing agent or exploiting a native radical on the sample of interest. Experiments are performed at a low temperature of ~ K with continuous microwave irradiations and benefit from the innovative low-temperature MAS probe that enables sample polarization in-situ, directly at the NMR field.As a spectroscopic method, nuclear magnetic resonance (NMR) has seen spectacular growth, both as a technique and in its applications.
Today's applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive coverage of the.